反应条件
water in N,N,N',N',N'',N''-hexamethylphosphoric triamide Equimolar mixt. of Et3GeLi and Me3SiGeEt2Li in HMPA is stirred for 94 h at 25°C, then Me3SiCl and water are added.; extn. with ether;
参考文献
Pigarev, S. D.; Bravo-Zhivotovskii, D. A.; Kalikhman, I. D.; Vyazankin, N. S.; Voronkov, M. G.
Journal of Organometallic Chemistry, 1989 , vol. 369, p. 29 - 42