water in toluene T=20°C; 27 h; Further byproducts given. Yields of byproduct given;
参考文献
Kopylov, V. M.; Agashkov, S. P.; Sunkovich, G. V.; Prikhod'ko, P. L.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -1,3 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of Me3SiCl; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 63 - 72
