in tetrahydrofuran byproducts: HCl, hexamethyldisiloxane; Room temperature, dropwise addn. with stirring of trimethylchlorosilane to slurry of metal salt.; Washing (hexane), evapn. at reduced pressure.;
N,N,N',N',N'',N''-hexamethylphosphoric triamide in toluene T=20°C; ΔG; Equilibrium constantThermodynamic data;
参考文献
Nilolaev, G. A.; Mileshkevich, V. P.; Vainshtein, P. M.; Shmeleva, O. A.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 9 p. 2098 - 2101,1867 - 1870
