1: 3,3-dimethylhexaethoxytrisiloxane With sodium hydroxide T=-35 - 15°C; 1.5 h; 2: chloro-trimethyl-silane in hexane Title compound not separated from byproducts;
1: meta-dibromobenzene With n-butyllithium in diethyl ether; hexane T=-54°C; 1.06667 h; 2: chloro-trimethyl-silane in diethyl ether; hexane T=-54 - 20°C;
参考文献
Stehouwer, Jeffrey S.; Jarkas, Nachwa; Zeng, Fanxing; Voll, Ronald J.; Williams, Larry; Owens, Michael J.; Votaw, John R.; Goodman, Mark M.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 23 p. 6760 - 6767
