in tetrahydrofuran Kinetics; under N2, to Me3SnSnMe3 added 1 M THF soln. of Me3SnLi, kept at room temp., at the predetermined times added Me3SiCl at -10°C; not isolated; detected by NMR and GLC;
1: furan With n-butyllithium in diethyl ether; hexane 3 h; Heating; 2: chloro-trimethyl-silane in diethyl ether; hexane T=25°C; 1 h;
参考文献
Raheem, Mohammed-Abdul; Tam, William
Synthetic Communications, 2013 , vol. 43, # 2 p. 260 - 267,8
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Raheem, Mohammed-Abdul; Tam, William
Synthetic Communications, 2013 , vol. 43, # 2 p. 260 - 267
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
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Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
