in tetrahydrofuran 1) DIPA, THF, -78°C; 2)TMSCl, room temp.;
参考文献
Harrowven, David C.; Curran, Dennis P.; Kostiuk, Sarah L.; Wallis-Guy, Ian L.; Whiting, Sally; Stenning, Kerri J.; Tang, Bencan; Packard, Emma; Nanson, Lana
Chemical Communications, 2010 , vol. 46, # 34 p. 6335 - 6337
in tetrahydrofuran Electrolysis; electrolysis carried out galvanostatically at 25-28°C in an atm.of dry N2, electrolyte 0.4 M LiClO4/THF; hexane added to electrolyte, ppt. filtered off, filtrate analyzed for product by GC, Bu3SnSiMe3 isolated in pure by chromy.;
in tetrahydrofuran Ar atmosphere, RYbI transferring dropwise under Ar pressure at room temperature, 2 to 3 h, Me3SnCl addn.; extracting with ether, extracts drying (Na2SO4);
参考文献
Russian Journal of General Chemistry, , vol. 67, # 1 p. 76 - 78
Bochkarev, L. N.; Kholodilova, M. N.; Zhil'tsov, S. F.; Guseva, T. V.; Bochkarev, M. N.; Razuvaev, G. A.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 642 - 643
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 723 - 724
