Komarov, N. V.; Ryzhkova, N. A.; Andreev, A. A.
Russian Chemical Bulletin, 1994 , vol. 43, # 2 p. 293 - 294
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 2 p. 313 - 314
in tetrahydrofuran
under N2 or Ar; mixture stirred for 15 h; pptn., solid separated by filtration,; IR spectrum of solid was consistent with the formulation MnCl2(thf), solvent evapd. under reduced pressure to leave liquid, warming at 40 ° C at 0.1 mm Hg gave Et2NCO2SiMe3, whose Ir spectrum was identical with that of an authentic sample;
参考文献
Belforte, Antonio; Calderazzo, Fausto; Zanazzi, Pier Francesco
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2921 - 2926
