反应条件
in diethyl ether
addition of CH3Li and n-C3F7I (formation of n-C3F7Li) to (CH3)3SiCl in ether at -30°C, heating to -18°C within 45 minutes, -10°C (15 minutes), 6°C (45 minutes);;
参考文献
McBee, E. T.; Roberts, C. W.; Judd, G. F.; Chao, T. S.
Proceedings of the Indiana Academy of Science, 1955 , vol. 65, p. 94 - 99
C. A., 1958 , p. 10870
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.7, page 17 - 32
