反应条件
tetrahydrofuran in tetrahydrofuran byproducts: CO, BF3*THF, Me3SiF; N2-atmosphere; slight molar excess of Me3SiCl, stirring (50°C, 30min); solvent removal, sublimation off of traces Mo(CO)6, extn. into CH2Cl2, filtration, evapn., washing (light petroleum, Et2O); elem. anal.;
参考文献
Bochmann, Manfred; Green, Michael; Kirsch, Howard P.; Stone, F. Gordon A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 714 - 718