water in water; toluene; butan-1-ol (CH3)2SiCl2 and (CH3)SiCl3 (1:1 mol) in butanol-H2O-toluene; heating of the oily product at 350-600°C in a slow stream of N2;; distn.; crystn. on cooling; recrystn. from toluene;;
Tamborski, C.; Post, H. W.
Journal of Organic Chemistry, 1952 , vol. 17, p. 1400 - 1404
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Gmelin Handbook: Si: MVol.C, 72, page 200 - 203
water in water; toluene; butan-1-ol (CH3)2SiCl2 and (CH3)SiCl3 (1:1 mol) in butanol-H2O-toluene; heating of the oily product at 350-600°C in a slow stream of N2;; distn.; crystn. on cooling; recrystn. from toluene;;