2,2,2-三氟乙醇合成路线 （共 1089 条）
反应条件
2,6-di-tert-butyl-4-methylpyridine; sodium carbonate; lithium bromide
1.) CH2Cl2, r.t., 2.) dioxane, water, 3 d, 120 deg C; MechanismProduct distribution;
参考文献
Bleckmann, Wolfgang; Hanack, Michael
Chemische Berichte, 1984 , vol. 117, # 10 p. 3021 - 3033
反应条件
acid in water
T=20 - 24°C; Product distribution;
参考文献
Richard, John P.; Rothenberg, Marc E.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1361 - 1372
参考文献
Brown,H.C.; Wetzel,C.R.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3724 - 3728
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Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
T=25°C; effect of 18-crown-6, Nα-NSb rearrangement of diazonium salt; Rate constantProduct distributionMechanism;
参考文献
Szele, Ivanka; Zollinger, Heinrich; Deshpande, Ashok D.
Helvetica Chimica Acta, 1981 , vol. 64, # 8 p. 2721 - 2727
反应条件
(i) Na, Et2O, (ii) (NPCl2)4; Multistep reaction;
参考文献
Allcock,H.R.; Walsh,E.J.
Journal of the American Chemical Society, 1972 , vol. 94, p. 119 - 124
反应条件
1.) 20 min., irradiation, 2.) 24 h, dark; Multistep reaction;
参考文献
Pavlik, James W.; Keil, Elinor B.; Sullivan, Eileen L.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 7 p. 1829 - 1834
反应条件
0.333333 h; Irradiationvar. time, concentration, other educts (alcohol solvents).; Product distributionMechanism;
参考文献
Pavlik, James W.; Keil, Elinor B.; Sullivan, Eileen L.
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 7 p. 1829 - 1834
反应条件
3.33333 h; Ambient temperatureIrradiation;
参考文献
Jaeger, David A.; Angelos, George H.
Tetrahedron Letters, 1981 , vol. 22, p. 803 - 806
反应条件
sodium azide; sodium perchlorate; water
T=70°C; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1383 - 1396
反应条件
sodium perchlorate; water
T=70°C; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1383 - 1396
