2,2,2-三氟乙醇合成路线 （共 1089 条）
参考文献
Bulletin of the Chemical Society of Japan, , vol. 75, # 4 p. 789 - 800
参考文献
Canning, Peter S. J.; Maskill, Howard; McCrudden, Katharine; Sexton, Brian
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 789 - 800
反应条件
Ambient temperatureIrradiation;
参考文献
Canning, Peter S. J.; McCrudden, Katharine; Maskill, Howard; Sexton, Brian
Chemical Communications, 1998 , # 18 p. 1971 - 1972
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
pyridine; phosphorus trichoride in diethyl ether 1.) -10 deg C, 1 h, 2.) reflux, 1 h;
参考文献
Leeuwen, P. W. N. M. van; Roobeek, C. F.
Tetrahedron, 1981 , vol. 37, p. 1973 - 1984
反应条件
phosphorus trichoride 1.) -5 deg C, 4 h, 2.) from -5 deg C to RT, 1 h;
参考文献
Luo; Atrazheva; Fregeau; Gmeiner; Lown
Canadian Journal of Chemistry, 1994 , vol. 72, # 6 p. 1548 - 1555
反应条件
other bis(fluoroalkyl) hydrogen phosphites; Mechanism;
参考文献
Mironov, V. F.; Konovalova, I. V.
Russian Journal of General Chemistry, 1993 , vol. 63, # 10.1 p. 1548 - 1550
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 10 p. 2228 - 2232
反应条件
potassium hydroxide in diethylene glycol dimethyl ether; water T=50°C; P=1500.15 Torr; 4.8 h; Cooling with liquid nitrogen; Product distribution / selectivity;
参考文献
ASAHI GLASS COMPANY LTD.
Patent: EP1655278 A1, 2006 ;
Location in patent: Page/Page column 8 ;
参考文献
Canning, Peter S. J.; Maskill, Howard; McCrudden, Katharine; Sexton, Brian
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 789 - 800
反应条件
phosphate buffer; N-hexadecyl-N,N,N-trimethylammonium bromide; sodium bromide T=25°C; pH=11.60; Kinetics;
参考文献
Tee; Yazbeck
Canadian Journal of Chemistry, 2000 , vol. 78, # 8 p. 1100 - 1108
