2,2,2-三氟乙醇合成路线 (共 1089 条)
反应条件
quinoline in pentane 7 h; Heating;
参考文献
Steinmetz, Mark G.; Yu, Changjun
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3107 - 3120
反应条件
T=5°C; 19 h; Irradiation; Rate constantQuantum yield;
参考文献
Steinmetz, Mark G.; Yu, Changjun
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3107 - 3120
反应条件
T=57.84°C; Gas phase; Equilibrium constant;
参考文献
Hurtado, Marcela; Yanez, Manuel; Herrero, Rebeca; Guerrero, Andres; Juan Z. Davalos; Jose-Luis, M. Abboud; Khater, Brahim; Guillemin, Jean-Claude
Chemistry - A European Journal, 2009 , vol. 15, # 18 p. 4622 - 4629
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Chung, Woo Jin; Welch, John T.
Journal of Fluorine Chemistry, 2004 , vol. 125, # 4 p. 543 - 548
反应条件
potassium fluoride; zirconium oxide T=140°C; 10 h; pressure tight reactor;
参考文献
Asahi Glass Co., Ltd.
Patent: EP2218708 A1, 2010 ;
Location in patent: Page/Page column 21; 22 ;
反应条件
triethylamine in N,N-dimethyl-formamide; 1,2-dichloro-benzene T=0 - 20°C;
参考文献
Bogolubsky, Andrey V.; Ryabukhin, Sergey V.; Pipko, Sergey E.; Lukin, Oleg; Shivanyuk, Alexander; Mykytenko, Dmytro; Tolmachev, Andrey
Tetrahedron, 2011 , vol. 67, # 20 p. 3619 - 3623
反应条件
pyridine in diethyl ether
参考文献
Krespan, Carl G.; Smart, Bruce E.
Journal of Organic Chemistry, 1986 , vol. 51, # 3 p. 320 - 326
反应条件
1: 2,2,2-trifluoroethanol With potassium hydroxide T=20°C; 1 h; 2: allyl bromide in water T=0°C;
参考文献
Audouard, Christophe; Garayt, Maxime R.; Kerouredan, Erwan; Percy, Jonathan M.; Yang, Hongli
Journal of Fluorine Chemistry, 2005 , vol. 126, # 4 p. 611 - 623
反应条件
potassium hydroxide in water T=40°C; 18 h;
参考文献
Audouard, Christophe; Fawcett, John; Griffith, Gerry A.; Kerouredan, Erwan; Miah, Afjal; Percy, Jonathan M.; Yang, Hongli
Organic Letters, 2004 , vol. 6, # 23 p. 4269 - 4272
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide T=40°C; 6 h;
参考文献
Boutevin, B.; Youssef, B.; Boileau, S.; Garnault, A. M.
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 399 - 410