2,2,2-三氟乙醇合成路线 （共 1089 条）
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 16 h; GloveboxInert atmosphere;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 60 h; GloveboxInert atmosphere;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 16 h; GloveboxInert atmosphere; Reagent/catalystSolventTimeTemperature;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 16 h; GloveboxInert atmosphere;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 16 h; GloveboxInert atmosphere;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
trans-[(2,6-bis(di-tert-butylphosphinomethyl)pyridine)Fe(H)2(CO)]; hydrogen; sodium methylate in 1,4-dioxane T=40°C; P=18751.9 Torr; 16 h; GloveboxInert atmosphere;
参考文献
Zell, Thomas; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2014 , vol. 53, # 18 p. 4685 - 4689
Angew. Chem., 2014 , vol. 126, # 18 p. 4773 - 4777
反应条件
hydrogen; anhydrous phosphine
反应条件
(Py)Zn(BH4)2 in tetrahydrofuran 1 h; Heating;
参考文献
Zeynizadeh, Behzad; Zahmatkesh, Karam
Journal of Chemical Research - Part S, 2003 , # 8 p. 522 - 525
反应条件
platinum(IV) oxide; diethyl ether T=90°C; Hydrogenation.unter Druck;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 43, p. 480
Chem. Zentralbl., , vol. 106, # I p. 549
Journal of the American Chemical Society, , vol. 70, p. 1281
反应条件
RuHCl(CO)(bis-(2-diphenylphosphinoethyl)amine); hydrogen; sodium methylate in methanol T=40°C; P=15201 Torr; 6 h; AutoclaveInert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 135, # 26 p. 9600 - 9603
