2,2,2-三氟乙醇合成路线 (共 1089 条)
反应条件
water T=100°C; autoclave;
参考文献
Burmakov, A. I.; Motnyak, L. A.; Kunshenko, B. V.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1204 - 1209
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1401 - 1408
反应条件
rhenium; water T=207°C; P=220652 Torr; Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 24, p. 1847,1852
反应条件
HCl in toluene titrn. calorimetric expt., titrn. of a soln. of Cp'2Zr(OCH2CF3)2 in toluene into a soln. of HCl in toluene; products not isolated, react. was monitored in prior expts. by NMR;
参考文献
Schock,L.E.; Marks,T.J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 7701
反应条件
in benzene T=20 - 25°C; 2 h;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 434 - 439
反应条件
sulfur(IV) fluoride T=160°C; 8 h; autoclave;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, # 7 p. 1204 - 1209
Zhurnal Organicheskoi Khimii, , vol. 16, # 7 p. 1401 - 1408
反应条件
methanol in dichloromethane T=10°C; 0.5 h; Irradiation; Product distribution;
参考文献
Brook; Balduzzi; Mohamed; Gottardo
Tetrahedron, 1999 , vol. 55, # 33 p. 10027 - 10040
反应条件
sodium tetrahydroborate in methanol T=20°C; 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 131, # 4 p. 477 - 486
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 70, p. 1968
反应条件
hydroxide in 1,4-dioxane; water T=50°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 8157 - 8163
反应条件
hydroxide in 1,4-dioxane; water T=50°C; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 8157 - 8163