2,2,2-三氟乙醇合成路线 (共 1089 条)
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
triethylamine; tetra-n-propylammonium bromide in water T=0 - 2°C; 3.2 h; Product distribution / selectivity;
参考文献
Central Glass Co., Ltd
Patent: JP2005/314356 A, 2005 ;
Location in patent: Page/Page column 9-10; 13 ;
反应条件
potassium carbonate; tetra-n-propylammonium bromide in water T=10.2 - 23.3°C; 4 - 7 h; Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 11; 13 ;
反应条件
potassium carbonate; triethylamine in water T=13.8 - 21°C; 4 - 5.5 h; Product distribution / selectivity;
参考文献
JP2005/314356 A, ;
Page/Page column 11-13 ;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
20°C for 48 h, after 110°C for 2.5 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
triethylamine in diethyl ether
参考文献
Balakrishna, M. S.; Prakasha, T. K.; Krishnamurthy, S. S.; Siriwardane, U.; Hosmane, N. S.
Journal of Organometallic Chemistry, 1990 , vol. 390, # 2 p. 203 - 216
反应条件
trifluorormethanesulfonic acid
参考文献
Endo, Yasuyuki; Shudo, Koichi; Okamoto, Toshihiko
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6393 - 6397
反应条件
caesium carbonate 20 h; UV-irradiation;
参考文献
Dichiarante, Valentina; Salvaneschi, Andrea; Protti, Stefano; Dondi, Daniele; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 51 p. 15919 - 15926
反应条件
Photolysis; Product distribution;
参考文献
Manet, Ilse; Monti, Sandra; Grabner, Gottfried; Protti, Stefano; Dondi, Daniele; Dichiarante, Valentina; Fagnoni, Maurizio; Albini, Angelo
Chemistry - A European Journal, 2008 , vol. 14, # 3 p. 1029 - 1039