2,2,2-三氟乙醇合成路线 (共 1089 条)
反应条件
4-ethyl-1-methyl-4H-[1,2,4]-triazol-1-ium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; 12 h; Solvent;
参考文献
Delany, Eoghan G.; Fagan, Claire-Louise; Gundala, Sivaji; Zeitler, Kirsten; Connon, Stephen J.
Chemical Communications, 2013 , vol. 49, # 58 p. 6513 - 6515
反应条件
iodine; potassium carbonate T=50°C; 5 h;
参考文献
Mori, Naoshi; Togo, Hideo
Tetrahedron, 2005 , vol. 61, # 24 p. 5915 - 5925
反应条件
boron trifluoride; toluene T=0°C;
参考文献
Prakash, G. K. Surya; Mathew, Thomas; Marinez, Eric R.; Esteves, Pierre M.; Rasul, Golam; Olah, George A.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3952 - 3958
反应条件
triethylamine in diethyl ether
参考文献
Liepin'sh, E. E.; Zitsmane, I. A.; Ignatovich, L. M.; Lukevits, E.; Guvanova, L. I.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1789 - 1792,1609 - 1612
反应条件
carbon monoxide; triethylamine in acetonitrile 10 atm CO, presence of Et3N, N2-atmosphere, mixing at -20°C, stirring for 1 h at 40°C; GC-anal., product selectivity detd.;
参考文献
Yamashita; Sakakura; Kobayashi; Tanaka
Journal of molecular catalysis, 1988 , vol. 48, # 1 p. 69 - 79
反应条件
triethylamine; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene T=100°C; P=15001.2 Torr; 24 h;
参考文献
Jimenez-Rodriguez, Cristina; Eastham, Graham R.; Cole-Hamilton, David J.
Dalton Transactions, 2005 , # 10 p. 1826 - 1830
反应条件
water T=25°C; variation of solvent system; Rate constantProduct distribution;
参考文献
Bentley, T. William; Koo, In Sun
Arkivoc, 2012 , vol. 2012, # 7 p. 25 - 34
反应条件
T=25°C; Solvolysis; Kinetics; Concentration;
参考文献
Bentley, T. William; Koo, In Sun
Arkivoc, 2012 , vol. 2012, # 7 p. 25 - 34
参考文献
Brey; Tarrant
Journal of the American Chemical Society, 1957 , vol. 79, p. 6533,6534,6536
反应条件
bis-[(trifluoroacetoxy)iodo]benzene 0.166667 h;
参考文献
Miyazawa, Etsuko; Sakamoto, Takeshi; Kikugawa, Yasuo
Heterocycles, 2003 , vol. 59, # 1 p. 149 - 160