2,2,2-三氟乙醇合成路线 （共 1089 条）
反应条件
T=20°C; Irradiation;
参考文献
Kirmse, Wolfgang; Krzossa, Birgit; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 32 p. 7473 - 7477
反应条件
Co(III)(salpr)(OH) in 1,2-dichloro-ethane
T=60°C; 8 h;
参考文献
Nishinaga; Ando; Maruyama; Mashino
Synthesis, 1992 , # 9 p. 839 - 841
反应条件
in water
T=30°C; solvolysis; further temperature; in absolute solvent; Rate constantProduct distribution;
参考文献
Hanack,M.; Auchter,G.
Journal of the American Chemical Society, 1985 , vol. 107, p. 5238
反应条件
caesium carbonate
19 h; Inert atmosphereIrradiation;
参考文献
Raviola, Carlotta; Protti, Stefano; Ravelli, Davide; Mella, Mariella; Albini, Angelo; Fagnoni, Maurizio
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9094 - 9101
反应条件
caesium carbonate
12 h; Inert atmosphereIrradiation;
参考文献
Raviola, Carlotta; Protti, Stefano; Ravelli, Davide; Mella, Mariella; Albini, Angelo; Fagnoni, Maurizio
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9094 - 9101
反应条件
in N,N-dimethyl-formamide
T=20°C; Schlenk techniqueInert atmosphere; Solvent;
参考文献
Soto, Marc; Comalrena, Helena; Balduzzi, Ursula; Guirado, Gonzalo; Lloveras, Vega; Vidal-Gancedo, Jose; Sebastian, Rosa Maria; Marquet, Jordi
Tetrahedron Letters, 2013 , vol. 54, # 47 p. 6310 - 6313
反应条件
oxygen; bis-aminomethyl-bis(8-hydroxyquinoline) cobalt(II)
T=20 - 165°C; P=3000.3 - 27002.7 Torr; autoclave; Product distribution / selectivity;
参考文献
Jacob, Andreas; Wershofen, Stefan; Klein, Stephan; Sundermeyer, Jorg; Mei, Fuming
Patent: US2009/275771 A1, 2009 ;
Location in patent: Page/Page column 13 ;
反应条件
tetraethylammonium bromide in acetonitrile
Ambient temperatureelectrochemically induced (Pt electrodes, 100 mA);
参考文献
Matsumura, Yoshihiro; Maki, Toshihide; Satoh, Yuki
Tetrahedron Letters, 1997 , vol. 38, # 51 p. 8879 - 8882
反应条件
4-methyl-morpholine
T=65°C; alcoholysis; Product distribution;
参考文献
Zhu, Jiang; Bennet, Andrew J.
Journal of Organic Chemistry, 2000 , vol. 65, # 14 p. 4423 - 4430
反应条件
sodium trifluoroethoxide
T=10 - 20°C; 0.5 h;
参考文献
Leitich, Johannes; Heise, Ingeborg
European Journal of Organic Chemistry, 2001 , # 14 p. 2707 - 2718
