2,2,2-三氟乙醇合成路线 (共 1089 条)
反应条件
triethylamine in diethyl ether
参考文献
Liepin'sh, E. E.; Zitsmane, I. A.; Ignatovich, L. M.; Lukevits, E.; Guvanova, L. I.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1789 - 1792,1609 - 1612
反应条件
triethylamine; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene
T=100°C; P=15001.2 Torr; 24 h;
参考文献
Jimenez-Rodriguez, Cristina; Eastham, Graham R.; Cole-Hamilton, David J.
Dalton Transactions, 2005 , # 10 p. 1826 - 1830
反应条件
potassium tert-butylate; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene
T=100°C; P=15001.2 Torr; 24 h;
参考文献
Jimenez-Rodriguez, Cristina; Eastham, Graham R.; Cole-Hamilton, David J.
Dalton Transactions, 2005 , # 10 p. 1826 - 1830
反应条件
water
T=25°C; Solvolysis; Kinetics; Concentration;
参考文献
Bentley, T. William; Koo, In Sun
Arkivoc, 2012 , vol. 2012, # 7 p. 25 - 34
反应条件
T=25°C; Solvolysis; Kinetics; Concentration;
参考文献
Bentley, T. William; Koo, In Sun
Arkivoc, 2012 , vol. 2012, # 7 p. 25 - 34
反应条件
perchloric acid; sodium perchlorate in water
T=22°C; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1373 - 1383
反应条件
perchloric acid; sodium perchlorate; water
T=22°C; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1373 - 1383
反应条件
perchloric acid; sodium perchlorate; water
T=22°C; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1373 - 1383
反应条件
1: With sodium hydroxide
T=20 - 60°C; 72 h;
2: With sulfuric acid in water
T=0°C;
参考文献
PFIZER LIMITED
Patent: WO2006/136917 A1, 2006 ;
Location in patent: Page/Page column 34 ;
WO 2006/136917 A1
反应条件
in water; toluene; mineral oil
参考文献
Chevron Research Company
Patent: US4846873 A1, 1989 ;