2,2,2-三氟乙醇合成路线 （共 1089 条）
反应条件
2,6-dimethylpyridine
T=70 - 73°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Creary,X.; Geiger,C.C.
Journal of the American Chemical Society, 1982 , vol. 104, p. 4151
反应条件
hydrogenchloride
T=25°C; Product distributionKinetics; Further Variations:Temperatures;
参考文献
Katzhendler, Jehoshua; Schneider, Hava; Ta-Shma, Rachel; Breuer, Eli
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 9 p. 1961 - 1968
反应条件
hydrogenchloride
T=25°C; Product distribution;
参考文献
Katzhendler, Jehoshua; Schneider, Hava; Ta-Shma, Rachel; Breuer, Eli
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 9 p. 1961 - 1968
反应条件
in tetrahydrofuran
T=20°C; 1 h;
参考文献
Mata, Graa; Do Rosario, Virgilio E.; Iley, Jim; Constantino, Luis; Moreira, Rui
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 2 p. 886 - 892
反应条件
in water
T=50°C; Rate constant;
参考文献
Nakashima, Tohru; Fujiyama, Ryoji; Fujio, Mizue; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 5 p. 1043 - 1047
反应条件
sodium azide; sodium perchlorate; water
T=22°C; other temp., other solvent; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1383 - 1396
反应条件
sodium azide; sodium perchlorate; water
T=22°C; other temp., other solvent; Product distribution;
参考文献
Richard, John P.; Jencks, William P.
Journal of the American Chemical Society, 1984 , vol. 106, # 5 p. 1383 - 1396
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=80°C; 2 h;
参考文献
Suzuki, Hideo; Fujimoto, Takuya; Yamamoto, Takeshi
Patent: US2010/190747 A1, 2010 ;
Location in patent: Page/Page column 43 ;
反应条件
sodium hydride in N,N-dimethyl-formamide
T=150°C; 15 h;
参考文献
Gupton, John T.; Hertel, George; DeCrescenzo, Gary; Colon, Cesar; Baran, Donna; et al.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 3037 - 3042
反应条件
in acetonitrile
UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4279 - 4282
