in tetrachloromethane byproducts: O2, acetone, tert-butanol; under Ar; addn. of peroxide to soln. of aluminum and germanium compds. in CCl4, stirred at room temp. for 30 min; qualitative analysis, chromy. detection, iodometric titration;
参考文献
Stepovik; Gulenova; Martynova; Skvortsov; Cherkasov
Russian Journal of General Chemistry, 2005 , vol. 75, # 7 p. 1098 - 1107
boron trifluoride diethyl etherate in pentane 1.) -5 deg C, 15 min, 2.) up to r.t.; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
boron trifluoride diethyl etherate in pentane 1.) -5 deg C, 15 min, 2.) up to r.t.; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
boron trifluoride diethyl etherate in pentane 1.) -5 deg C, 15 min, 2.) up to r.t.; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
in octane T=10 - 50°C; 0.00138889 h; k(eff), E(eff), preexponential factor, W0Σ, contribution of protolysis γ; Rate constantThermodynamic data;
参考文献
Alyasov, V. N.; Maslennikov, V. P.; Aleksandrov, Yu. A.; Kuznetsov, I. Yu.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 5 p. 1139 - 1145,996 - 1003