1-苯甲酰基-1-溴环己烷合成路线 （共 8 条）
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride T=80°C; 1 h;
参考文献
Meneguzzo, Enzo; Norcini, Gabriele; Li Bassi, Giuseppe
Patent: US2011/65962 A1, 2011 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; toluene
参考文献
Tchoubar
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 720
反应条件
1: methanol; sodium tetrahydroborate / 0 °C / Inert atmosphere 2: diethylzinc; trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme
参考文献
Wang, Zhihui; Li, Meiyi; Zhang, Wenqin; Jia, Jiangnan; Wang, Fei; Xue, Song
Tetrahedron Letters, 2011 , vol. 52, # 45 p. 5968 - 5971
反应条件
sodium hydroxide; toluene
参考文献
Tchoubar
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1952 , vol. 235, p. 720
反应条件
bromine; hydrogen bromide in water; acetic acid
T=25°C; stereoelectronic effects; Rate constant;
参考文献
Pollack, Ralph M.; Kayser, Robert H.; Cashen, Michael J.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3983 - 3987
反应条件
1: AlCl3, aluminium chloride / 1.33 h / 10 - 60 °C
2: sodium hypochlorite; hydrogen bromide / water / 2.5 h / 60 - 100 °C
View Scheme
参考文献
Meneguzzo, Enzo; Norcini, Gabriele; Li Bassi, Giuseppe
Patent: US2011/65962 A1, 2011 ;
反应条件
1: AlCl3, aluminium chloride / 1.33 h / 10 - 60 °C
2: sodium hypochlorite; hydrogen bromide / water / 2.5 h / 60 - 100 °C
View Scheme
参考文献
Meneguzzo, Enzo; Norcini, Gabriele; Li Bassi, Giuseppe
Patent: US2011/65962 A1, 2011 ;
反应条件
1: methanol.
2: diethyl ether
View Scheme
参考文献
Stevens; Farkas
Journal of the American Chemical Society, 1952 , vol. 74, p. 618
