反应条件
1: 64 percent / diisobutylaluminium hydride / benzene / 0.25 h / 10 °C
2: 83 percent / Et3N / CH2Cl2 / 1 h / 0 °C
3: 16 percent / t-BuOK / tetrahydrofuran / 0.5 h / 20 °C
4: solid / 0.33 h / 15 - 20 °C / Irradiation; photolysis of benzene solution; photochemistry and rearrangements of bicyclo<3.1.0>hex-3-en-2-ones; solution photolysis, solution behavior; solid-state photolysis, crystal lattice behavior
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参考文献
Zimmerman; Sebek
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3677 - 3690