吗啉基(4-甲氧基苯基)甲酮合成路线 （共 28 条）
反应条件
bromobenzene; potassium carbonate; triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether
24 h; Heating;
参考文献
Tamaru, Yoshinao; Yamada, Yoshimi; Yoshida, Zen-ichi
Synthesis, 1983 , # 6 p. 474 - 476
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran
T=20°C; 2 h;
参考文献
Lemoucheux; Rouden; Lasne
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9997 - 10001
反应条件
dichlorophenyl phosphine oxide in acetonitrile
T=-4°C; 2.5 h;
参考文献
Kim, Yong Hae; Lim, Sang Chul; Chang, Hae Sung
Journal of the Chemical Society, Chemical Communications, 1990 , # 1 p. 36 - 37
反应条件
tert.-butylhydroperoxide; FeCl3·6H2O in water; acetonitrile
Inert atmosphereReflux;
参考文献
Porcheddu, Andrea; Luca, Lidia De
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 2949 - 2953,5
Title/Abstract Show Details
Porcheddu, Andrea; Luca, Lidia De
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 16 p. 2949 - 2953
反应条件
1: morpholine With Sm(III) chloride; lithium hexamethyldisilazane in tetrahydrofuran
T=20°C;
2: methyl 4-(N-tert-butoxycarbonyl-(5S)-methyl-(2S)-pyrrolidinylmethoxy)benzoate in tetrahydrofuran
T=0°C;
参考文献
Campbell, James B.; Sparks, Richard B.; Dedinas, Robert F.
Synlett, 2011 , # 3 art. no. S08010ST, p. 357 - 360
反应条件
pyridine
T=70°C; 5 h; Inert atmosphere;
参考文献
McNulty, James; Vemula, Ramesh; Krishnamoorthy, Venkatesan; Robertson, Al
Tetrahedron, 2012 , vol. 68, # 27-28 p. 5415 - 5421
反应条件
in tetrahydrofuran; hexane
T=0°C; 0.166667 h; Inert atmosphere;
参考文献
Park, Jae Kyo; Shin, Won Kyu; An, Duk Keun
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 5 p. 1592 - 1594
反应条件
potassium carbonate; 1,1'-bis(diphenylphosphino)ferrocene; [(Pd(.mu.-Cl)(.kappa.(2)-P,C-P(OC6H2-2,4-tBu2)(OC6H3-2,4-tBu2)2))2] in 1,4-dioxane
T=120°C; P=6750.54 Torr; 14 h;
参考文献
Fairlamb, Ian J. S.; Grant, Stephanie; McCormack, Peter; Whittall, John
Dalton Transactions, 2007 , # 8 p. 859 - 865
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; triphenylphosphine in toluene
T=140°C; 20 h;
参考文献
Tillack, Annegret; Rudloff, Ivo; Beller, Matthias
European Journal of Organic Chemistry, 2001 , # 3 p. 523 - 528
反应条件
triethylamine in dichloromethane
T=20°C; 1 h;
参考文献
Kang, Dong Ho; Joo, Tae Young; Lee, Eun Hwa; Chaysripongkul, Skaydaw; Chavasiri, Warinthorn; Jang, Doo Ok
Tetrahedron Letters, 2006 , vol. 47, # 32 p. 5693 - 5696
