反应条件
1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C
1.2: 16 h / -78 - 25 °C
2.1: toluene-4-sulfonic acid / water; toluene / 16 h / 20 - 25 °C
3.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C
3.2: 16 h / -78 - 25 °C
4.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1 h
5.1: toluene / 16 h / Reflux
View Scheme
参考文献
Joannesse, Caroline; Morrill, Louis C.; Campbell, Craig D.; Slawin, Alexandra M. Z.; Smith, Andrew D.
Synthesis, 2011 , # 12 art. no. C43011SS, p. 1865 - 1879
