1-(2-氨基-4-吡啶基)-2-溴乙烷酮合成路线 （共 4 条）
反应条件
water; hydrogen bromide; bromine; acetic acid
T=70°C; 2 h;
参考文献
Green, Jeremy; Cao, Jingrong; Bandarage, Upul; Come, Jon; Marhefka, Craig
Patent: US2007/270386 A1, 2007 ;
Location in patent: Page/Page column 35 ;
反应条件
1: diethyl ether
2: bromine; aq. HBr; acetic acid / 0.5 h / 70 °C
View Scheme
参考文献
Bandarage, Upul K.; Come, Jon H.; Green, Jeremy
Tetrahedron Letters, 2006 , vol. 47, # 46 p. 8079 - 8081
反应条件
1: DMA / 1 h / 130 °C
2: diethyl ether
3: bromine; aq. HBr; acetic acid / 0.5 h / 70 °C
View Scheme
参考文献
Bandarage, Upul K.; Come, Jon H.; Green, Jeremy
Tetrahedron Letters, 2006 , vol. 47, # 46 p. 8079 - 8081
反应条件
hydrogen bromide; bromine; acetic acid
T=70°C; 0.5 h;
参考文献
Bandarage, Upul K.; Come, Jon H.; Green, Jeremy
Tetrahedron Letters, 2006 , vol. 47, # 46 p. 8079 - 8081
