2-溴-5-甲氧基苯甲醛合成路线 （共 53 条）
反应条件
1: N-bromosuccinmide / acetonitrile / 20 °C 2: pyridinium chlorochromate / dichloromethane / 20 °C View Scheme
参考文献
Dalton Transactions, , vol. 42, # 2 p. 355 - 358
反应条件
water; calcium carbonate 24 h; Heating;
参考文献
Rosillo, Marta; Dominguez, Gema; Casarrubios, Luis; Amador, Ulises; Perez-Castells, Javier
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2084 - 2093
反应条件
1: 69 percent / Fe; HCl 2: t-BuONO; HBr 3: CuBr View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 37 p. 6589 - 6592
反应条件
1: t-BuONO; HBr 2: CuBr View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 37 p. 6589 - 6592
参考文献
Justus Liebigs Annalen der Chemie, , vol. 391, p. 44
反应条件
1: 1.) Zn, PPh3 / 1.) CH2Cl2, RT, 30 min, 2.) CH2Cl2, 1.5 h 2: 98 percent / Pd(PPh3)4, n-Bu3SnH / toluene / 1 h / Ambient temperature View Scheme
参考文献
Tietze, Lutz F.; Noebel, Thomas; Spescha, Maurus
Journal of the American Chemical Society, 1998 , vol. 120, # 35 p. 8971 - 8977
反应条件
1: Jones reagent View Scheme
参考文献
Dell'Acqua, Monica; Abbiati, Giorgio; Arcadi, Antonio; Rossi, Elisabetta
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7836 - 7848
反应条件
1: NaBH4 / tetrahydrofuran / 4 h / 0 °C 2: CBr4; PPh3 / acetonitrile / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 37 p. 6941 - 6945
反应条件
1.1: 89 percent / p-toluenesulfonic acid / toluene / 15 h / Heating 2.1: n-BuLi / diethyl ether; hexane / 0.75 h / -78 °C 2.2: B(OBu)3 / -78 - 20 °C 2.3: 81 percent / H2O; H+ / 2 h / 25 °C View Scheme
参考文献
Speicher, Andreas; Groh, Matthias; Hennrich, Markus; Huynh, Anh-Minh
European Journal of Organic Chemistry, 2010 , # 35 p. 6760 - 6778
反应条件
1: 99 percent / HONH2*HCl; aq. NaOH / ethanol / 12 h / 23 °C 2: 87 percent / 2-chloro-1,3-dimethylimidazolium chloride; Et3N / CH2Cl2 / cooling View Scheme
参考文献
Mello, Jesse V.; Finney, Nathaniel S.
Journal of the American Chemical Society, 2005 , vol. 127, # 29 p. 10124 - 10125
