2-溴-5-甲氧基苯甲醛合成路线 （共 53 条）
反应条件
1: tetrahydrofuran / 3 h / 0 - 20 °C / |Inert atmosphere
2: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C / |Inert atmosphere
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参考文献
Mahendar, Lodi; Satyanarayana, Gedu
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2059 - 2074
反应条件
1: 100 percent / CsF / Pd(PPh3)4 / 1,2-dimethoxy-ethane / 20 h / Heating
2: 96 percent / NaOH, (n-Bu)NI, water / 96 h / Heating
3: 56 percent / Me3SO3H / CHCl3 / 2 h / Ambient temperature
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参考文献
Kumar, Subodh
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 19 p. 3157 - 3161
反应条件
1: 57 percent / K2CO3 / Cu / dimethylformamide / 6 h / 150 °C
2: 1) Mg / 1) THF; 2) THF, reflux, 4 h
3: 1.22 g / NaH / dimethylformamide / 11 h / 70 °C
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参考文献
Sindelar; Metysova; Holubek; et al.
Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 11 p. 3077 - 3093
