1-(2,6-二羟基-4-甲氧基苯基)乙酮合成路线 (共 24 条)
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 70 °C
2: potassium hydroxide / ethanol
3: boron trichloride / dichloromethane / 0 °C
View Scheme
参考文献
Chen, Yau-Hung; Wang, Wei-Hua; Wang, Yun-Hsin; Lin, Zi-Yu; Wen, Chi-Chung; Chern, Ching-Yuh
Molecules, 2013 , vol. 18, # 2 p. 2052 - 2060
反应条件
boric acid in toluene
T=120°C; 48 h;
参考文献
Chan, Wing Lai; Lin, Yong Cheng; Zhang, Wei Han; Tang, Pak Lai; Szeto, Yau Shan
Heterocycles, 1996 , vol. 43, # 3 p. 551 - 554
反应条件
ethylenediamine diacetic acid in xylene
10 h; Heating;
参考文献
Yong, Rok Lee; Xia, Likai
Synthesis, 2007 , # 20 p. 3240 - 3246
反应条件
1: 0.6 g / orthophosphoric acid / petroleum ether / 2 h / 30 - 35 °C
2: 0.065 g / DDQ / benzene / 8 h / Heating
View Scheme
参考文献
Ahluwalia, V. K.; Jain, Anjula; Goyal, Madhuri
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 2 p. 166 - 167