Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
1: 100 percent Spectr. / CH2Cl2 / 1 h / 0 °C
2: acetyl bromide / acetonitrile
3: 95 percent / benzene / 7 h / Heating
4: phosgene / benzene / a) 0 deg C, 30 min, b) RT, 30 h
5: H2O / tetrahydrofuran / 0.5 h
View Scheme
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
1: acetyl bromide / acetonitrile
2: 95 percent / benzene / 7 h / Heating
3: phosgene / benzene / a) 0 deg C, 30 min, b) RT, 30 h
4: H2O / tetrahydrofuran / 0.5 h
View Scheme
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
1: 95 percent / benzene / 7 h / Heating
2: phosgene / benzene / a) 0 deg C, 30 min, b) RT, 30 h
3: H2O / tetrahydrofuran / 0.5 h
View Scheme
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
Corrie, John E. T.; Trentham, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2409 - 2418
hydrogenchloride in water
1 h; Heating; Yield given;
参考文献
Corrie, John E. T.; Trentham, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2409 - 2418
1: 1.) 1H tetrazole, 2.) m-chlorperbenzoic acid / 1.) THF, r.t., 1 h, 2.) THF, CH2Cl2, 0 deg C, 1 h
2: 0.1 N methanolic NaOH / 1 h / 50 °C
3: conc. HCl / H2O / 1 h / Heating
View Scheme
参考文献
Corrie, John E. T.; Trentham, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2409 - 2418
1: 0.1 N methanolic NaOH / 1 h / 50 °C
2: conc. HCl / H2O / 1 h / Heating
View Scheme
参考文献
Corrie, John E. T.; Trentham, David R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2409 - 2418
in water; acetonitrile
Irradiationvar. solvents ratio; pH 2 and pH 7; Quantum yield;
参考文献
Givens, Richard S.; Athey, Phillip S.; Matuszewski, Bogdan; Kueper III, L. William; Xue, Jie-You; Fister, Thomas
Journal of the American Chemical Society, 1993 , vol. 115, # 14 p. 6001 - 6012
