9H-芴-9-酮(三苯基膦)腙合成路线 （共 18 条）
反应条件
in dichloromethane
T=40°C; 1.83333 h;
参考文献
LANXESS DEUTSCHLAND GMBH
Patent: US2009/76226 A1, 2009 ;
Location in patent: Page/Page column 16-17 ;
反应条件
(i) Br2, benzene, (ii) /BRN= 1910575/, Et3N; Multistep reaction;
参考文献
Bestmann,H.J.; Fritzsche,H.
Chemische Berichte, 1961 , vol. 94, p. 2477 - 2485
反应条件
(2-hydroxyphenyl)oxoacetic acid in toluene
T=20°C; 24 h;
参考文献
Staudinger; Luescher
Helvetica Chimica Acta, 1922 , vol. 5, p. 84
反应条件
sodium in tetrahydrofuran
0.75 h;
参考文献
Handoo, Kishan L.; Gadru, Kanchan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 412 - 417
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
Product distribution;
参考文献
Herbranson, Dale E.; Theisen, F. J.; Hawley, M. Dale; McDonald, Richard N.
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2544 - 2549
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
Product distribution;
参考文献
Herbranson, Dale E.; Theisen, F. J.; Hawley, M. Dale; McDonald, Richard N.
Journal of the American Chemical Society, 1983 , vol. 105, # 9 p. 2544 - 2549
反应条件
oxygen; methylene blue in dichloromethane
T=-78°C; 0.0833333 h; Irradiationother reagent;
参考文献
Suzuki, Nobutaka; Wakatsuki, Satoshi; Izawa, Yasuji
Tetrahedron Letters, 1980 , vol. 21, p. 2313 - 2314
反应条件
lead dioxide in dichloromethane
T=30°C; 1.33333 h;
参考文献
Handoo, Kishan L.; Gadru, Kanchan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 412 - 417
