1,2,3,4-四苯基萘合成路线 (共 86 条)
反应条件
in solid matrix Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, placing th cell into a quartz windowed Dewar filled with liquid N2, irradn. with a low-pressure mercury lamp (254 nm) at 77K in 3-methylpentane matrix, warming to room temp., recooling to 77K; detd. by UV;
参考文献
Organometallics, , vol. 8, p. 2759 - 2766
参考文献
Ando, Wataru; Itoh, Hiroyuki; Tsumuraya, Takeshi
Organometallics, 1989 , vol. 8, p. 2759 - 2766
反应条件
in solid matrix Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, placing th cell int aquartz windowed Dewar filled with liquid N2, irradn. with a low-pressure mercury lamp (254 nm) at 77K in 3-methylpentane matrix, warming to room temp., recooling to 77K; not isolated, detd. by UV;
参考文献
Organometallics, , vol. 8, p. 2759 - 2766
反应条件
in solid matrix Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, placing the cell into a quartz windowed Dewar filled with liquid N2, irradn. with a low-pressure mercury lamp (254 nm) at 77K for 5-30min., warming to room temp., recooling to 77K, 3-MP matrix; not isolated, detd. by UV;
参考文献
Organometallics, , vol. 8, p. 2759 - 2766
反应条件
in solid matrix Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, placing th cell int aquartz windowed Dewar filled with liquid N2, irradn. with a low-pressure mercury lamp (254 nm) at 77K in 3-methylpentane matrix , warming to room temp., recooling to 77K; not isolated, detd. by UV;
参考文献
Organometallics, , vol. 8, p. 2759 - 2766
反应条件
tetrahydrofuran; 2-fluorophenylmagnesium bromide
参考文献
Chemische Berichte, , vol. 91, p. 895,899
参考文献
Ando, Wataru; Hamada, Yoshitaka; Sekiguchi, Akira
Journal of the Chemical Society, Chemical Communications, 1982 , # 14 p. 787 - 788
参考文献
Chemical Communications (London), , p. 744 - 745
Journal of the Chemical Society [Section] C: Organic, , p. 819 - 824
反应条件
in tetrachloromethane Elimination; Photolysis;
参考文献
Russian Chemical Bulletin, , vol. 49, # 3 p. 421 - 426
参考文献
Journal of Organic Chemistry, , vol. 40, # 7 p. 883 - 889