N-乙酰-D-氨基葡萄糖合成路线 (共 161 条)
反应条件
pyridine; acetic anhydride
参考文献
KOTOBUKI PHARMACEUTICAL CO., LTD.
Patent: US2002/107224 A1, 2002 ;
反应条件
pyridine; calcium sulfate anschliessend Erwaermen mit Acetanhydrid;
参考文献
Anderson; Percival
Journal of the Chemical Society, 1956 , p. 819,822
反应条件
acetyl chloride T=20 - 50°C; 6 h; Inert atmosphere;
参考文献
Yamaguchi, Takao; Blazquez, Blas; Hesek, Dusan; Lee, Mijoon; Llarrull, Leticia I.; Boggess, Bill; Oliver, Allen G.; Fisher, Jed F.; Mobashery, Shahriar
ACS Medicinal Chemistry Letters, 2012 , vol. 3, # 3 p. 238 - 242
反应条件
hydrogenchloride T=85°C; 2 h; Title compound not separated from byproducts;
参考文献
, vol. 1986, # 1 p. 37 - 45
反应条件
in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 42, # 43 p. 7567 - 7570
参考文献
Bornaghi, Laurent; Dekany, Gyula; Drinnan, Nicholas Barry; Papageorgiou, John; West, Michael Leo
Patent: US2004/58888 A1, 2004 ;
反应条件
sodium hypochlorite; phosphate buffer in water T=37°C; Oxidation; pH=7.4; 6 h; Product distribution;
参考文献
Jahn, Michael; Baynes, John W.; Spiteller, Gerhard
Carbohydrate Research, 1999 , vol. 321, # 3-4 p. 228 - 234
参考文献
Vila Pahi, Francisco Javier; Flores Salgado, Francesc; Ruhi Roura, Ramon; Arnau Pastor, Narcis
Patent: US2003/181400 A1, 2003 ;
反应条件
Amberlite IR 120 (H) resin 16 h; Heating;
参考文献
Gao, Feng; Yan, Xuxu; Shakya, Tushar; Baettig, Oliver M.; Ait-Mohand-Brunet, Samia; Berghuis, Albert M.; Wright, Gerard D.; Auclair, Karine
Journal of Medicinal Chemistry, 2006 , vol. 49, # 17 p. 5273 - 5281
反应条件
Dowex HCR-W2 (H+) resin 1 h; Reflux;
参考文献
Journal of the American Chemical Society, , vol. 132, # 13 p. 4641 - 4652