N-乙酰-D-氨基葡萄糖合成路线 （共 161 条）
参考文献
Cornforth et al.
Biochemical Journal, 1958 , vol. 68, p. 57,59
反应条件
1: 20 °C 2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C 3: acetone / |Reflux View Scheme
参考文献
Nakamura, Motomi; Tsutsumi, Mayuka; Ishikawa, Yoshiaki; Umemiya, Haruka; Izawa, Kazumi; Abe, Haruka; Togashi, Yosuke; Kinone, Tatsuya; Sekiguchi, Sho; Igumi, Mihiro; Ide, Kanako; Hasegawa, Teruaki; Hasegawa, Toki
Tetrahedron, 2013 , vol. 69, # 14 p. 3019 - 3026
反应条件
1: 20 °C 2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C 3: acetone / |Reflux View Scheme
参考文献
Nakamura, Motomi; Tsutsumi, Mayuka; Ishikawa, Yoshiaki; Umemiya, Haruka; Izawa, Kazumi; Abe, Haruka; Togashi, Yosuke; Kinone, Tatsuya; Sekiguchi, Sho; Igumi, Mihiro; Ide, Kanako; Hasegawa, Teruaki; Hasegawa, Toki
Tetrahedron, 2013 , vol. 69, # 14 p. 3019 - 3026
反应条件
1: 100 percent / CH3COCl / 23 h 2: 35 percent / p-TsOH / dimethylformamide / 2.5 h / 70 °C View Scheme
参考文献
Organic and biomolecular chemistry, , vol. 1, # 21 p. 3826 - 3838
反应条件
hydrogenchloride T=85°C; 2 h; Title compound not separated from byproducts;
参考文献
McGuigan, Christopher; Serpi, Michaela; Bibbo, Rita; Roberts, Helen; Hughes, Clare; Caterson, Bruce; Gibert, Ana Torrent; Verson, Carlos Raul Alaez
Journal of Medicinal Chemistry, 2008 , vol. 51, # 18 p. 5807 - 5812
反应条件
in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Bera, Smritilekha; Linhardt, Robert J.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3181 - 3193
反应条件
sodium azide; 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine in water T=0°C; 1 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 12, # 6 p. 942 - 955
反应条件
1: 20 °C 2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C 3: acetone / |Reflux View Scheme
参考文献
Nakamura, Motomi; Tsutsumi, Mayuka; Ishikawa, Yoshiaki; Umemiya, Haruka; Izawa, Kazumi; Abe, Haruka; Togashi, Yosuke; Kinone, Tatsuya; Sekiguchi, Sho; Igumi, Mihiro; Ide, Kanako; Hasegawa, Teruaki; Hasegawa, Toki
Tetrahedron, 2013 , vol. 69, # 14 p. 3019 - 3026
反应条件
1: 35 percent / trimethylsilyl chloride / 0.5 h / 60 - 80 °C
2: 495 mg / H2 / Pd(OH)2/C / methanol / 1.5 h / 20 °C
View Scheme
参考文献
Sasaki, Kenji; Nishida, Yoshihiro; Kambara, Mikie; Uzawa, Hirotaka; Takahashi, Tadanobu; Suzuki, Takashi; Suzuki, Yasuo; Kobayashi, Kazukiyo
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 6 p. 1367 - 1375
参考文献
Zilliken et al.
Archives of Biochemistry, 1955 , vol. 54, p. 398,402
