N-乙酰-D-氨基葡萄糖合成路线 (共 161 条)
反应条件
cis-5-hydroxy-1,3-dioxane; Thermus thermophilus β-galactosidase in aq. phosphate buffer T=60°C; pH=6; 3 h; Enzymatic reaction; ConcentrationReagent/catalyst; regioselective reaction;
参考文献
Tetrahedron, , vol. 69, # 3 p. 1148 - 1152
反应条件
β-galactosidase from Bacillus circulans in aq. phosphate buffer T=23°C; pH=7.3; Ionic liquidEnzymatic reaction; SolventTemperature;
参考文献
Kaftzik, Nicole; Wasserscheid, Peter; Kragl, Udo
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 553 - 557
反应条件
in water Bacillus circulans β-galactosidase presence;
参考文献
Range, Gerhard; Kraehmer, Ralf; Welzel, Peter; Mueller, Dietrich; Herrmann, Guido F.; Kragl, Udo; Wandrey, Christian; Markus, Astrid; Van Heijenoort, Yveline; Van Heijenoort, Jean
Tetrahedron, 1997 , vol. 53, # 5 p. 1695 - 1706
反应条件
1.1: 20 °C 1.2: 44 percent / K2CO3 / acetone / 55 °C 2.1: 97 percent / NaOCH3; MeOH / CHCl3 View Scheme
参考文献
Chen, Hong-Ming; Withers, Stephen G.
Carbohydrate Research, 2007 , vol. 342, # 15 p. 2212 - 2222
反应条件
inorganic pyrophosphatase cloned from Pasteurella multocida strain P-1059; N-acetylglucosamine-1-phosphate uridylyltransferase cloned from Pasteurella multocida strain P-1059 (ATCC15742); N-acetylhexosamine 1-kinase cloned from Bifidobacterium longum ATCC55813; adenosine 5'-triphosphoric acid; magnesium chloride in water T=37°C; pH=8; aq. bufferEnzymatic reaction;
参考文献
Chen, Yi; Thon, Vireak; Li, Yanhong; Yu, Hai; Ding, Li; Lau, Kam; Qu, Jingyao; Hie, Liana; Chen, Xi
Chemical Communications, 2011 , vol. 47, # 38 p. 10815 - 10817
反应条件
1: N-acetylglucosamine kinase (GlcK, C. albicans) 2: N-acetylglucosamine phosphate mutase (Agm1, S. cerevisiae) 3: 92 percent / GlcNAc; PEP; ATP / Glc-1,6-dP1; MgCl2 / various solvents / 20 h View Scheme
参考文献
Shao, Jun; Zhang, Jianbo; Nahalka, Jozef; Wang, Peng George
Chemical Communications, 2002 , # 21 p. 2586 - 2587
反应条件
1: With hydrogenchloride T=20°C; 17 h; 2: With sodium hydrogencarbonate
参考文献
Zilliken et al.
Archives of Biochemistry, 1955 , vol. 54, p. 398,402
反应条件
1: 20 °C 2: acetic anhydride; hydrogen bromide; acetic acid / dichloromethane / 20 °C 3: acetone / |Reflux View Scheme
参考文献
Nakamura, Motomi; Tsutsumi, Mayuka; Ishikawa, Yoshiaki; Umemiya, Haruka; Izawa, Kazumi; Abe, Haruka; Togashi, Yosuke; Kinone, Tatsuya; Sekiguchi, Sho; Igumi, Mihiro; Ide, Kanako; Hasegawa, Teruaki; Hasegawa, Toki
Tetrahedron, 2013 , vol. 69, # 14 p. 3019 - 3026
反应条件
1-methyl-pyrrolidin-2-one; Wilkinson's catalyst T=110 - 125°C; 22 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 22 p. 5257 - 5264
反应条件
pyridine 1.) Bacillus circulans β-galactosidase presence, water, 2.) 20 deg C, 4 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 53, # 5 p. 1695 - 1706