2-[(4-硝基苯甲酰基)氨基]乙酸乙酯合成路线 (共 18 条)
反应条件
triethylamine in 1,4-dioxane 4 h; Ambient temperature; Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 619 - 621
反应条件
1,1'-carbonyldiimidazole 1) DMF, 0 deg C -> room temperature, 20 min, 2) DMF, room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1539 - 1545
参考文献
Chemische Berichte, , vol. 36, p. 1648
反应条件
in water; dimethyl sulfoxide T=25°C; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 76, # 6 p. 729 - 737
反应条件
1: With sodium hydroxide in mthanol T=0 - 20°C; 2: With acetic acid in methanol
参考文献
F2G LTD
Patent: WO2008/62182 A1, 2008 ;
Location in patent: Page/Page column 153 ;
反应条件
hydrogenchloride in water Inert atmosphere;
参考文献
Barnett, Derek W.; Refaei, Maryanne S.; Curley Jr., Robert W.
Journal of Labelled Compounds and Radiopharmaceuticals, 2013 , vol. 56, # 1 p. 6 - 11
反应条件
ammonium hydroxide
0.5 h;
参考文献
Woll, Matthew G.; Hadley, Erik B.; Mecozzi, Sandro; Gellman, Samuel H.
Journal of the American Chemical Society, 2006 , vol. 128, # 50 p. 15932 - 15933
反应条件
potassium hydroxide; hydroxylamine hydrochloride in methanol
Ambient temperature; Yield given;
参考文献
Munakata; Tanaka; Toyoshima
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 7 p. 2045 - 2051