反应条件
1: 54 percent / pyridinium chlorochromate/NaOAc / CH2Cl2 / 2.5 h / Ambient temperature
2: 1. Mg / 1. THF 2. THF/room temperature/overnight, then 2 h/reflux
3: 77 percent / aq. HCl / acetone / 2 h
4: 1. Mg / 1. Et2O 2. Et2O/room temperature/overnight
5: 50 percent / Jones' reagent / acetone
View Scheme
参考文献
Vig, O. P.; Sharma, S. D.; Soni, B. R.; Sharma, M. L.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 5 p. 353 - 355
