3-甲氧基-1,2-二甲基-9H-咔唑-4-醇合成路线 （共 24 条）
反应条件
1: 1.) Hg(OAc)2, AcOH, 2.) BH3*THF, 3.) alkaline H2O2
2: 95 percent / K2CO3 / acetone / Heating
3: 4-dimethylaminopyridine / acetonitrile
4: 95 percent / N-bromosuccinimide / acetonitrile
5: 1.) BuLi, 2.) B(OMe)3, 3.) alkaline H2O2
6: 98 percent / 180 - 190 °C
View Scheme
参考文献
Moody, Christopher J.; Shah, Pritom
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 376 - 377
反应条件
1: 95 percent / N-bromosuccinimide / acetonitrile
2: 1.) BuLi, 2.) B(OMe)3, 3.) alkaline H2O2
3: 98 percent / 180 - 190 °C
View Scheme
参考文献
Moody, Christopher J.; Shah, Pritom
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 376 - 377
反应条件
1: 1.) BuLi, 2.) B(OMe)3, 3.) alkaline H2O2
2: 98 percent / 180 - 190 °C
View Scheme
参考文献
Moody, Christopher J.; Shah, Pritom
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 376 - 377
反应条件
potassium carbonate in acetone
Heating;
参考文献
Moody, Christopher J.; Shah, Pritom
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 376 - 377
