N-(4-甲基亚苄基)-4-甲基苯磺酰胺合成路线 (共 30 条)
反应条件
N-chloro-succinimide; tin(ll) chloride in dichloromethane T=-40 - 20°C; 25 h;
参考文献
Masuyama, Yoshiro; Yamamoto, Naoko; Kurusu, Yasuhiko
Synlett, 2002 , # 12 p. 2113 - 2115
反应条件
boron trifluoride diethyl etherate in toluene T=20°C; 7.5 h;
参考文献
Akiyama, Takahiko; Sugano, Megumi; Kagoshima, Hirotaka
Tetrahedron Letters, 2001 , vol. 42, # 23 p. 3889 - 3892
反应条件
in tetrahydrofuran T=25°C;
参考文献
Fan, Renhua; Pu, Dongming; Wen, Fengqi; Wu, Jie
Journal of Organic Chemistry, 2007 , vol. 72, # 23 p. 8994 - 8997
反应条件
monoethoxy-diethylaluminum in tetrahydrofuran T=0 - 20°C; 15 h; Title compound not separated from byproducts;
参考文献
Bejot, Romain; Anjaiah, Siddam; Falck; Mioskowski, Charles
European Journal of Organic Chemistry, 2007 , # 1 p. 101 - 107
反应条件
Gd(OTf)3 T=20°C; 6 h;
参考文献
Temelli, Baris; Unaleroglu, Canan
Tetrahedron, 2006 , vol. 62, # 43 p. 10130 - 10135
反应条件
trimethoxy silane; lithium methanolate in tetrahydrofuran
59 h; Ambient temperature;
参考文献
Hojo, Makoto; Murakami, Chikara; Fujii, Atsuko; Hosomi, Akira
Tetrahedron Letters, 1999 , vol. 40, # 5 p. 911 - 914
反应条件
hydrogenchloride; samarium in tetrahydrofuran
T=20°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Liu, Xi; Liu, Yunkui; Zhang, Yongmin
Tetrahedron Letters, 2002 , vol. 43, # 38 p. 6787 - 6789
反应条件
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in chloroform; water
4 h; further sulfonimines; MechanismProduct distribution;
参考文献
Davis, Franklin A.; Lamendola, Joseph; Nadir, Upender; Kluger, Edward W.; Sedergran, Thomas C.; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2000 - 2005
反应条件
in toluene
T=120°C; 12 h; Inert atmosphere; optical yield given as percent de;
参考文献
Yan, Yizhe; Xu, Kun; Fang, Yang; Wang, Zhiyong
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6849 - 6855
反应条件
1: 72 percent / 2.5M BuLi / hexane; tetrahydrofuran / 4 h / -78 °C
2: 45 percent / NaOH / ethanol / 12 h / 90 °C
View Scheme
参考文献
Katritzky; Li; Gordeev
Synthesis, 1994 , # 1 p. 93 - 96