7,8-二羟基-3-(4-羟基苯基)苯并吡喃-4-酮合成路线 （共 4 条）
反应条件
boron trifluoride diethyl etherate; methanesulfonyl chloride T=80°C; 3 h;
参考文献
Xiao, Zhu-Ping; Shi, Da-Hua; Li, Huan-Qiu; Zhang, Li-Na; Xu, Chen; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 11 p. 3703 - 3710
反应条件
methanesulfonyl chloride in N,N-dimethyl-formamide T=60 - 70°C; 1 h;
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
反应条件
1: 92 percent / BF3*Et2O / 1 h / 60 - 70 °C 2: 83 percent / methanesulphonyl chloride / dimethylformamide / 1 h / 60 - 70 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 3005 - 3008
反应条件
1: 92 percent / BF3*Et2O / 1 h / 60 - 70 °C 2: 83 percent / methanesulphonyl chloride / dimethylformamide / 1 h / 60 - 70 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 3005 - 3008
