1-溴-1,2,3,4-四氢萘合成路线 (共 5 条)
反应条件
bromine; 1,2-bis-(diphenylphosphino)ethane in dichloromethane
T=-15 - 20°C; Bromination;
参考文献
Braslau, Rebecca; Naik, Neeta; Zipse, Hendrik
Journal of the American Chemical Society, 2000 , vol. 122, # 35 p. 8421 - 8434
参考文献
Cakmak, Osman; Kahveci, Ismail; Demirtas, Ibrahim; Hoekelek, Tuncer; Smith, Keith
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 11 p. 1791 - 1804
参考文献
Abbott GmbH and Co., KG
Patent: US6740647 B1, 2004 ;
Location in patent: Page column 27 ;
US 6740647 B1
反应条件
styrene-4-vinyl(N-alkylpyridinium bromide) in water; acetic acid
T=23°C; 24 h;
参考文献
Zajc, Barbara; Zupan, Marko
Tetrahedron, 1989 , vol. 45, # 24 p. 7869 - 7878
反应条件
1: sodium tetrahydroborate / ethanol / Inert atmosphere
2: hydrogen bromide / dichloromethane; water
View Scheme
参考文献
Sun, Ke; Liu, Sheng; Bec, Patryk M.; Driver, Tom G.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 7 p. 1702 - 1706