4-甲基四氢-2H-吡喃-4-醇合成路线 （共 15 条）
反应条件
sulfuric acid
T=40 - 80°C; Kinetics;
参考文献
Ryvkina; Sinitsyn
Russian Journal of Applied Chemistry, 1998 , vol. 71, # 8 p. 1479 - 1481
反应条件
toluene-4-sulfonic acid in benzene
3 h; Heating;
参考文献
Chini, Marco; Crotti, Paolo; Gardelli, Cristina; Macchia, Franco
Tetrahedron, 1994 , vol. 50, # 4 p. 1261 - 1274
反应条件
potassium hydrogensulfate
T=140 - 150°C; 1 h; distillation;
参考文献
Booth, Harold; Kheidhair, Kheidhair A.; Readshaw, Simon A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4699 - 4724
反应条件
hydrogen bromide; lithium bromide in water
T=0 - 20°C;
参考文献
Dudnik, Alexander S.; Fu, Gregory C.
Journal of the American Chemical Society, 2012 , vol. 134, # 25 p. 10693 - 10697
反应条件
1: 57 percent / potassium hydrogen sulphate / 1 h / 140 - 150 °C / distillation
2: hydrogen / 10percent Pd/C / 3 h / 760 Torr / Ambient temperature
View Scheme
参考文献
Booth, Harold; Kheidhair, Kheidhair A.; Readshaw, Simon A.
Tetrahedron, 1987 , vol. 43, # 20 p. 4699 - 4724
