2-乙酰基-3,4-二氢-5,8-二甲氧基萘合成路线 (共 27 条)
反应条件
aluminium trichloride in dichloromethane
T=0°C; 0.5 h;
参考文献
Badalassi, Fabrizio; Crotti, Paolo; Di Bugno, Cristina; D'Arata, Fabio; Favero, Lucilla; Ramacciotti, Alessio
Tetrahedron Asymmetry, 2001 , vol. 12, # 22 p. 3155 - 3161
反应条件
N-chloro-succinimide; silver nitrate in water; acetonitrile
0.333333 h; Ambient temperature;
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Rao, B. Ramamohan; Ravichandran, K.
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1115 - 1116
反应条件
sodium hydroxide in methanol
12 h; Heating;
参考文献
Russell; Collin; Crane; et al.
Australian Journal of Chemistry, 1984 , vol. 37, # 8 p. 1721 - 1728
反应条件
formic acid
T=100 - 110°C; 2 h;
参考文献
Tanno; Terashima
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 811 - 820
反应条件
in diethyl ether
3 h; Ambient temperature;
参考文献
Terashima, Shiro; Tanno, Norihiko; Koga, Kenji
Tetrahedron Letters, 1980 , vol. 21, p. 2749 - 2752
反应条件
1: 85 percent / BF3 etherate
2: HCl gas / CHCl3 / 10 h / Ambient temperature
3: 76 percent / NaBH4 / methanol / 24 h / Ambient temperature
4: 73 percent / NCS, AgNO3 / acetonitrile; H2O / 0.33 h / Ambient temperature
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Rao, B. Ramamohan; Ravichandran, K.
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1115 - 1116
反应条件
dipyridinium dichromate
参考文献
Reddy, M. Parameswara; Rao, G. S. Krishna
Tetrahedron Letters, 1981 , vol. 22, # 36 p. 3549 - 3550
反应条件
Yield given. Multistep reaction;
参考文献
Suzuki; Kimura; Terashima
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 11 p. 3559 - 3572
反应条件
1: HCl gas / CHCl3 / 10 h / Ambient temperature
2: 76 percent / NaBH4 / methanol / 24 h / Ambient temperature
3: 73 percent / NCS, AgNO3 / acetonitrile; H2O / 0.33 h / Ambient temperature
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Rao, B. Ramamohan; Ravichandran, K.
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1115 - 1116
反应条件
1: 76 percent / NaBH4 / methanol / 24 h / Ambient temperature
2: 73 percent / NCS, AgNO3 / acetonitrile; H2O / 0.33 h / Ambient temperature
View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Rao, B. Ramamohan; Ravichandran, K.
Tetrahedron Letters, 1982 , vol. 23, # 10 p. 1115 - 1116