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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
75272-81-0
合成路线
（共 6 条）
4430-41-5
→
反应条件
75272-81-0
反应条件
sodium periodate in 1,4-dioxane; water
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
629-41-4
1,8-辛二醇
→
反应条件
75272-81-0
反应条件
1: 42percent HBr 2: methanol 3: 86 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran 4: 69 percent / NH2NH2*H2O / ethanol 5: 89 percent / dicyclohexylcarbodiimide / diethyl ether; tetrahydrofuran 6: 81 percent / sodium metaperiodate / H2O; dioxane View Scheme
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
98958-45-3
→
反应条件
75272-81-0
反应条件
1: 89 percent / dicyclohexylcarbodiimide / diethyl ether; tetrahydrofuran 2: 81 percent / sodium metaperiodate / H2O; dioxane View Scheme
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
98957-86-9
→
反应条件
75272-81-0
反应条件
1: 86 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran 2: 69 percent / NH2NH2*H2O / ethanol 3: 89 percent / dicyclohexylcarbodiimide / diethyl ether; tetrahydrofuran 4: 81 percent / sodium metaperiodate / H2O; dioxane View Scheme
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
50816-19-8
8-溴-1-辛醇
→
反应条件
75272-81-0
反应条件
1: methanol 2: 86 percent / diethyl azodicarboxylate, triphenylphosphine / tetrahydrofuran 3: 69 percent / NH2NH2*H2O / ethanol 4: 89 percent / dicyclohexylcarbodiimide / diethyl ether; tetrahydrofuran 5: 81 percent / sodium metaperiodate / H2O; dioxane View Scheme
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
59501-76-7
→
反应条件
75272-81-0
反应条件
1: 69 percent / NH2NH2*H2O / ethanol 2: 89 percent / dicyclohexylcarbodiimide / diethyl ether; tetrahydrofuran 3: 81 percent / sodium metaperiodate / H2O; dioxane View Scheme
参考文献
Kawabata, Jun; Fukushi, Yukiharu; Hayashi, Ryoko; Suzuki, Ken; Mishima, Yoshio; et al.
Agricultural and Biological Chemistry, 1989 , vol. 53, # 12 p. 3361 - 3362
