反应条件
1: 92 percent / NaIO4 / methanol; H2O / MCPBA, ether, 0 deg C
2: 93 percent / Ac2O, MsOH / CH2Cl2 / E:Z ratio= 2:1
3: 1.) t-BuOK / 1.) THF, -78 to 0 deg C
View Scheme
参考文献
Durman, John; Hunt, Paul G.; Warren, Stuart
Tetrahedron Letters, 1983 , vol. 24, # 20 p. 2113 - 2116
