反应条件
zinc/copper couple in tetrahydrofuran; toluene Ar atmosphere, addn. of soln. of MeI to Cu/Zn, filtration, cooling (-30°C), addn. of Me2SnCl2 in THF/toluene (1:1) (dropwise, stirring, 2 h), stirring, (50°C, 12 h), solvent removed; dissolving (toluene), washing (HCl), drying (over Na2SO4), filtration, distn. (0.1 Torr); elem. anal.;
参考文献
Schumann, Herbert; Mohtachemi, Reza; Schwichtenberg, Michael
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1988 , vol. 43, # 11 p. 1510 - 1513
