n-butyllithium in tetrahydrofuran; diethyl ether boiling, 12h;;
参考文献
Ursino, J. A.
Diss. Abstr. B, Diss. St. John's Univ. 1967, 99 S. 1968 , vol. 28, p. 3662
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Kupchik, E. J.; Ursino, J. A.; Boudjouk, P. R.
Journal of Organometallic Chemistry, 1967 , vol. 10, p. 269 - 278
in dichloromethane Kinetics; -38.5 to -14.9°C, addn. of weak bases (nitromethane-d3, benzonitrile, acetonitrile-d3, dimethylacetamide, DMSO-d6); detected by NMR;
参考文献
Siddiqi, K. S.; Kureshy, R. I.; Khan, P.; Zaidi, S. A. A.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1983 , vol. 22, # 7 p. 616 - 617
in not given N2; cooling a flask with aryl-Grignard reagent to -78°C, addn. ofsolid Sn compd. (0.5 equiv.), stirring at -78°C for 20 min, warm ing to room temp., stirring over several hs.; removal of volatiles under reduced pressure, addn. of hexanes, filtration (Celite), washing the solid with hexanes, concg. the combined organic soln.;
参考文献
Thomas, J. Christopher; Peters, Jonas C.
Inorganic Chemistry, 2003 , vol. 42, # 17 p. 5055 - 5073
