反应条件
in isopropyl alcohol; benzene strictly anhydrous conditions; addn. of Na to excess of i-PrOH, refluxing (0.5 h), cooling, addn. of oxime, refluxing (2 h), cooling, addn. of stoichiom. amt. of Sn compound in benzene, refluxing (2 h); sovent removal (reduced pressure), filtration off of NaCl, crystn. (benzene/petroleum ether); elem. anal.;
参考文献
Singh; David Raju; Tiwari
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 10 p. 1711 - 1721
