反应条件
in not given
N2; cooling a flask with aryl-Grignard reagent to -78°C, addn. ofsolid Sn compd. (0.5 equiv.), stirring at -78°C for 20 min, warm ing to room temp., stirring over several hs.; removal of volatiles under reduced pressure, addn. of hexanes, filtration (Celite), washing the solid with hexanes, concg. the combined organic soln., standing until the oil is solidified;
参考文献
Thomas, J. Christopher; Peters, Jonas C.
Inorganic Chemistry, 2003 , vol. 42, # 17 p. 5055 - 5073
