反应条件
1: hexamethyl-silane With methyllithium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
cooling;
2: cyclohexenon in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
T=-78°C; 0.166667 h; Further stages.;
参考文献
Chow, Leonie; McClure, Melanie; White, Jonathan
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 5 p. 648 - 650